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HP 5890 Series II Plus Reference Manual Manual pdf 41 page image

HP 5890 Series II Plus Reference Manual

Also see for 5890 Series II: Service manual

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Contents
  1. Table Of Contents
  2. Table Of Contents
  3. Table Of Contents
  4. Table Of Contents
  5. Table Of Contents
  6. Chapter 1 — Columns and Fittings
  7. Column oven
  8. Column placement
  9. Hewlett•Packardcapillary columns
  10. Fittings
  11. Liners/adapters and inserts, general
  12. Inlet/detector liners/adapters
  13. Detector liners/adapters
  14. ECD and TCD adapters
  15. Liner/adapter installation
  16. Inlet inserts
  17. Split/splitless or split•onlycapillary inlet inserts
  18. Jet replacement, FIDs or NPDs
  19. Chapter 2 — Keyboard and Displays
  20. Displaying setpoints
  21. Entering setpoints
  22. Keyboard operation, INET control
  23. Protecting setpoints
  24. Loading default setpoints
  25. Chapter 3 — Temperature Control
  26. temperature control
  27. Valid setpoint ranges
  28. Cryogenic (sub•ambient)oven control
  29. Programming oven temperature
  30. Oven status
  31. Oven safety
  32. Fault: messages
  33. After a power failure
  34. Oven temperature calibration
  35. Chapter 4 — Electronic Flow Sensing
  36. Displaying gas flow rate
  37. Designating gas type
  38. Electronic flow sensor (EFS) calibration
  39. Preparation
  40. Setting the GAIN calibration value
  41. Entering specific ZERO and GAIN values
  42. Chapter 5 — Signal Output
  43. Zeroing signal output
  44. Signal attenuation
  45. Switching off the +1 mV output
  46. Test signal output
  47. Instrument network (INET)
  48. An instrument
  49. Active workspace
  50. INET operation
  51. Automatic INET reconfiguration
  52. Switching between Global and Local
  53. INET/HP•ILaddresses
  54. HP•ILloopback test
  55. Warn: and fault: messages
  56. File compatibility with data handling devices
  57. How do I change modes
  58. How to convert HP 339X Integrator workfiles from 5890A to SERIES II mode
  59. Chapter 6 — Inlet Systems
  60. Packed column inlet
  61. Electronic flow sensor
  62. Septum•purgedpacked column inlet
  63. Problems at high inlet temperatures
  64. Septum purge
  66. Split/splitless capillary inlet
  67. Carrier gas considerations
  68. Initial column head pressure
  69. Split sampling
  70. Splitless sampling
  71. Injection technique, split/splitless sampling
  72. Chapter 7 — Detector Systems
  73. Capillary makeup gas flow rate
  74. FID and NPD jets
  75. Flame ionization detector (FID)
  76. FID flameout problems
  77. Performance considerations
  78. Electron capture detector (ECD)
  79. Temperature
  80. Background level
  81. Thermal conductivity detector (TCD)
  82. Optimizing performance
  83. Analyzing for hydrogen, special considerations
  84. TCD•to•FID series connection
  85. Capillary column considerations
  86. Flame photometric detector (FPD)
  87. Flame ignition problems
  88. Chapter 8 — Preventive Maintenance
  89. Conditioning columns
  90. Re)Packing columns
  91. Changing septa
  92. Insert/liner care
  93. Cleaning
  94. Split/splitless capillary inlets
  95. Insert care
  96. Leaks
  98. Liner and/or insert care
  99. Repacking a split insert
  100. Metal inserts and/or liners
  101. Jet exchange/replacement
  103. Ignition problems
  105. Removing/replacing the NPD collector
  106. Type B NPD transformer/collector assembly
  107. Reinstallation
  108. Frequency test
  110. Thermal cleaning
  111. Packed column
  112. Radioactivity leak test (wipe test)
  113. Flame photometric detector
  114. Cleaning/replacing the FPD jet
  115. FPD leak testing (GC with electronic flow sensor)
  116. FPD leak testing (GC without electronic flow sensor)
  117. Conditioning chemical traps
  118. Chapter 9 — Chromatographic Troubleshooting
  119. Introduction
  120. Wander and drift
  121. Noise
  122. Spiking
  123. Retention time symptoms
  124. Peak symptoms
  125. Deformed peaks
  126. Troubleshooting valve systems
  127. Locating leaks
  128. Pressure check
  129. Electronic pressure control
  130. Safety shutdown
  131. Proper configuration
  132. Switch setting examples
  133. Chapter 10 — Test Sample Chromatograms
  134. test sample chromatograms
  135. Test sample chromatograms
  136. Index
HP 5890 Series II Plus Reference Manual Manual pdf 41 page image
Keyboard and DisplaysLoading default setpoints41Note that if the battery protecting memory should fail when main poweris turned off, the default setpoints are loaded into memory when thebattery is replaced. In addition, calibration constants for oventemperature control and gas flow rate monitoring are also reset to defaultvalues.
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5890 Series II5890 Series II Plus
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