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HP 5973 MSD Hardware Manual Manual pdf 35 page image

HP 5973 MSD Hardware Manual

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Contents
  1. Table Of Contents
  2. Table Of Contents
  3. Table Of Contents
  4. Specifications
  5. Reagent gases and regulators
  6. Hardware Reference
  7. CI ion source
  8. Reagent gas flow control module
  9. EI/CI GC/MSD interface (CI interface)
  10. Chemical Ionization Theory
  11. Chemical ionization overview
  12. Positive CI theory
  13. Negative CI theory
  14. CI setup
  15. To remove the CI MSD covers
  16. To pump down the MSD
  17. To install the GC column in the EI/CI GC/MSD interface
  18. To switch from CI to EI operating mode
  19. To switch from EI to CI operating mode
  20. To install the CI ion source
  21. To install the CI interface tip seal
  22. CI operation
  23. To set up the software for CI operation
  24. To set up methane reagent gas flow
  25. To perform CI autotune
  26. To perform a positive CI autotune (methane only)
  27. To perform a negative CI autotune (any reagent gas)
  28. To verify positive CI performance
  29. To verify negative CI performance
  30. To operate the reagent gas flow control module
  31. To monitor high vacuum pressure
  32. To use other reagent gases
  33. Troubleshooting tips and tricks
  34. Air leaks
  35. Pressure-related symptoms (overview)
  36. Poor vacuum without reagent gas flow
  37. High pressure with reagent gas flow
  38. Pressure does not change when reagent flow is changed
  39. Signal-related symptoms (overview)
  40. No peaks
  41. No or low reagent gas signal
  42. No or low PFDTD signal, but reagent ions are normal
  43. Excessive noise or low signal-to-noise ratio
  44. Tuning-related symptoms (overview)
  45. Reagent gas ion ratio is difficult to adjust or unstable
  46. High electron multiplier voltage
  47. Can not complete autotune
  48. Peak widths are unstable
  49. To clean the CI ion source
  50. To minimize foreline pump damage from ammonia
  51. To replace the methane/isobutane gas purifier
  52. To refill the CI calibrant vial
  53. To purge the CI calibration valve
  54. To connect the vacuum gauge controller
  55. To clean the reagent gas supply lines (tubing)
  56. GC/MSD interface parts
  57. CI ion source parts
  58. Flow control module parts
  59. Ferrules
  60. Miscellaneous parts
/ 122
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This manual is suitable for:
5973 MSD