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HP 5973 Hardware Manual Manual pdf 153 page image

HP 5973 Hardware Manual

Also see for 5973: Hardware installation manual

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Contents
  1. Table Of Contents
  2. Table Of Contents
  3. Table Of Contents
  4. Table Of Contents
  5. Table Of Contents
  6. Table Of Contents
  7. Table Of Contents
  8. Side
  9. High
  10. To prepare a capillary column for installation
  11. To install a capillary column in a split/splitless inlet
  12. To condition a capillary
  13. To install a capillary column without the installation tool
  14. To install a capillary column using the installation tool
  15. Main
  16. To view MSD analyzer temperature and vacuum status
  17. To set monitors for MSD temperature and vacuum status
  18. To set the MSD analyzer temperatures
  19. To set the interface temperature from the ChemStation
  20. To monitor high vacuum pressure
  21. To measure column flow linear velocity
  22. To calculate column flow
  23. To set the interface temperature from an HP 6890 GC
  24. To remove the MSD covers
  25. Power cord
  26. To open the vacuum manifold
  27. To close the vacuum manifold
  28. To pump down the MSD
  29. To connect the optional gauge controller
  30. To move or store the MSD
  31. To vent the MSD without the ChemStation
  32. General
  33. Primary
  34. MSD is on but the status LEDs are all
  35. Poor
  36. Peaks are
  37. Baseline is
  38. Retention times for all peaks drift –
  39. High abundances at m/z 18, 28, 32, and 44 or at m/z 14 and
  40. Peak widths are
  41. High mass sensitivity is
  42. Foreline pressure is too
  43. Gauge controller displays 9.9+9 and then goes
  44. Power indicator on the gauge controller does not
  45. Temperature symptoms
  46. Mass filter (quad) heater will not heat up
  47. Error messages
  48. Difficulty with the fan
  49. Turbomolecular pump
  50. Temperature control disabled
  51. The system is in vent state
  52. Air leaks
  53. Contamination
  54. Before starting
  55. Maintaining the vacuum system
  56. To check and add foreline pump oil
  57. To drain the foreline pump
  58. To refill the foreline pump
  59. To replace the oil trap
  60. To check the diffusion pump fluid
  61. To separate the MSD from the GC
  62. To remove the diffusion pump
  63. To replace the diffusion pump fluid
  64. To reinstall the diffusion pump
  65. To reconnect the MSD to the GC
  66. To remove the calibration vial
  67. To refill and reinstall the calibration vial
  68. To remove the foreline gauge
  69. To reinstall a foreline gauge
  70. To remove the calibration valve
  71. To reinstall a calibration valve
  72. To replace the fan for the high vacuum pump
  73. To remove the triode gauge tube
  74. To reinstall a triode gauge tube
  75. To lubricate the side plate O-ring
  76. To lubricate the vent valve O-ring
  77. Maintaining the analyzer
  78. To remove the ion source
  79. To disassemble the ion source
  80. To clean the ion source
  81. To reassemble the ion source
  82. To reinstall the ion source
  83. To remove a filament
  84. To reinstall a filament
  85. To remove the heater and sensor from the ion source
  86. To reinstall the heater and sensor in the ion source
  87. To remove the heater and sensor from the mass filter
  88. To reinstall the heater and sensor in the mass filter
  89. To replace the electron multiplier horn
  90. Maintaining the GC/MSD interface
  91. To remove the GC/MSD interface heater and sensor
  92. To reinstall the GC/MSD interface heater and sensor
  93. Maintaining the electronics
  94. To adjust the RF coils
  95. To replace the primary fuses
  96. Diffusion pump MSD vacuum system
  97. Turbo pump MSD vacuum system
  98. Diffusion pump vacuum manifold
  99. Turbo pump vacuum manifold
  100. Side plate
  101. Vacuum seals
  102. High voltage feedthrough seal
  103. Foreline pump
  104. Foreline gauge
  105. Diffusion pump and fan
  106. Turbomolecular pump and fan
  107. Calibration valve and vent valve
  108. Triode gauge tube
  109. Gauge controller
  110. Ion source
  111. Filaments
  112. Emission current
  113. Filament care
  114. Drawout plate and cylinder
  115. Mass filter
  116. AMU offset
  117. DC polarity
  118. Quadrupole maintenance
  119. Signal amplifier
  120. Analyzer heaters and radiators
  121. Back panel and
  122. Low voltage (ac-dc) power
  123. Pumpdown safety
  124. Remote start
  125. Remote control
  126. Power status
  127. Electronics
  128. Vacuum system
  129. Analyzer
  130. GC/MSD interface
  131. Consumables and maintenance supplies
  132. High vacuum signal ( HIVAC SIGNAL )
HP 5973 Hardware Manual Manual pdf 153 page image
4 Maintaining the MSDTo clean the ion source1538 Dry the cleaned parts in an oven at 100 ° – 150 °C for 30 minutes.Take care to avoid recontaminating cleaned and dried parts. Put on new, cleangloves before handling the parts. Do not set the cleaned parts on a dirty surface.Set them only on clean, lint-free cloths.: $ 5 1 , 1 * /HWWKHVHSDUWVFRROEHIRUH\RXKDQGOHWKHP
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